HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoyl chloride → N-Propylbenzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoyl chloride | HCID 7412 | — |
| Reactant | Propylamine | HCID 7852 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | N-Propylbenzamide | HCID 25354 | 96% |
Reaction Steps
Benzoyl chloride (10 mL, 86.2 mmol) in ethyl acetate (200 mL) was treated with propylamine. The precipitate was removed by filtration, and the solution was washed with 1M HCl, 5% NaHCO3, and brine, dried over MgSO4 and concentrated in vacuo to give the title compound in 96% yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05631401 |
| Source dataset | uspto-grants-1997_05 |
| ORD ID | ord-39484ed599c04b63b91693a7e1f09678 |
| Source note | uspto-grants-1997_05 |