HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyrrole → HCID 10678999, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyrrole | HCID 8027 | — |
| Reactant | 4-(Bromomethyl)benzonitrile | HCID 86996 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 10678999 | HCID 10678999 | — |
Reaction Steps
Using pyrrole and 4-(bromomethyl)benzonitrile and the method of Example 53A, except using DMF as the solvent, provided N-(4-cyanobenzyl)pyrrole. 1H NMR (CDCl3) δ 7.62 (m, 2H), 7.14 (m, 2H), 6.69 (m, 2H), 6.24 (m, 2H), 5.15 (s, 2H). MS (DCl/NH3) m/e 183 (M+H)+, 200 (M+H+NH3)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05631401 |
| Source dataset | uspto-grants-1997_05 |
| ORD ID | ord-a164abf20dbc49c9b6d478b635237038 |
| Source note | uspto-grants-1997_05 |