HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Phenoxybenzaldehyde → HCID 19048166, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Phenoxybenzaldehyde | HCID 66139 | — |
| Reactant | (2-(Methylthio)ethyl)amine | HCID 87697 | — |
| Product | HCID 19048166 | HCID 19048166 | 93% |
Reaction Steps
Following the procedure described in Example 68A, 4-phenoxybenzaldehyde (1.98 g, 10 mmol) and 2-methylthioethylamine (0.912 g, 10 mmol) were combined to give the title compound (2.53 g, 93%) 1H NMR (300 MHz, CDCl3) δ 7.32 (m, 4 H), 7.09. (t, 1 H), 6.97 (m, 4 H), 3.80 (s, 2 H), 2.84 9t, 2 H), 2.68 (t, 2 H), 2.10 (s, 3 H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05631401 |
| Source dataset | uspto-grants-1997_05 |
| ORD ID | ord-9f45dad8c60d489d95c63e01bee5ba95 |
| Source note | uspto-grants-1997_05 |