Hydrochloric Acid → HCID 67711044, compound

Participants

Reaction Steps

The crystals of compound 4 obtained above are suspended in ethanol. An ethanolic solution of hydrogen chloride gas is then added: the base dissolves and the hydrochloride then begins to precipitate out. After cooling and dilution with ethyl ether, the crystals are filtered off and then washed with a 50/50 ethanol/ethyl ether mixture, and then with ethyl ether. After drying, 4.25 g (yield 80%) of compound 5 are recovered in the form of white crystals.

Provenance & Evidence