HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 19045469, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 19045229 | HCID 19045229 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 19045469 | HCID 19045469 | — |
Reaction Steps
The product of Step B (0.5 g) in CH3OH (15 mL) and 6N HCl (15 mL) was heated at reflux for 10 hours. The reaction was concentrated to dryness. and the residue flushed with ethanol (4 times) and then toluene to yield 0.5 g of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05633247 |
| Source dataset | uspto-grants-1997_05 |
| ORD ID | ord-e0c45232d4d140a19e8b3300f46045d5 |
| Source note | uspto-grants-1997_05 |