Phenylglyoxylic Acid → HCID 10200352, compound

HRID 1781472Notes

Reaction equation

HRID 1781472 reaction equation
CC(C1C=CC=C(C(C)C)C=1CC([C:16]1[C:17]([CH:30]([CH3:32])[CH3:31])=[C:18]([O:25][S:26](=[O:29])(=[O:28])[NH2:27])[C:19]([CH:22]([CH3:24])[CH3:23])=[CH:20][CH:21]=1)=O)C.C(C1C=CC=C(C(C)C)C=1CC(O)=O)(C)C.[C:49]([C:57]([OH:59])=O)(=[O:56])[C:50]1[CH:55]=[CH:54][CH:53]=[CH:52][CH:51]=1>>[O:56]=[C:49]([C:50]1[CH:51]=[CH:52][CH:53]=[CH:54][CH:55]=1)[C:57]([C:16]1[C:17]([CH:30]([CH3:32])[CH3:31])=[C:18]([O:25][S:26](=[O:28])(=[O:29])[NH2:27])[C:19]([CH:22]([CH3:24])[CH3:23])=[CH:20][CH:21]=1)=[O:59]

Participants

4

Reactant 3

HCID 11915Phenylglyoxylic AcidHCID 10226443Sulfamic acid[[2,6-bis(1-methylethyl)phenyl]-acetyl]-2,6-bis(1-methylethyl)phenyl esterHCID 152779902-(2,6-Diisopropylphenyl)acetic acid

Product 1

HCID 10200352HCID 10200352, compound

Procedure

This compound was prepared in the same manner as for the title compound of Example 1, except that 2,6-diisopropylphenylacetic acid was replaced with benzoylformic acid, mp 106°-109° C.

Sources & evidence

ORD record
ord-499982a4b04547d4972e2ae6e3a13543
Source dataset
uspto-grants-1997_05
Patent number
US05633287

Reaction notes

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