HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86750886, compound → HCID 70303321, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86750886 | HCID 86750886 | — |
| Solvent | Methylenechloride Hexane | HCID 21226440 | — |
| Product | HCID 70303321 | HCID 70303321 | — |
Reaction Steps
By following the procedure of Example ZA-6A and substituting methyl (E)-6-(1,3-dihydro-4-hydroxy-6-methoxy-7-methyl-3-oxoisobenzofuran-5-yl) 2,4-dimethyl-4-hexenoate with ethyl (E)-6-(1,3-dihydro-4-hydroxy-6-methoxy-7-methyl-3-oxoisobenzofuran-5-yl)-3-methoxy-4-methyl-4-hexenoate and the corresponding compounds of Formula I-ZA-M1 prepared as described in Part A above, there are obtained (E)-6-(1,3-dihydro-4-hydroxy-6-methoxy-7-methyl-3-oxoisobenzofuran-5-yl)-3-methoxy-4-methyl-4-hexenoic acid, m.p. 133°-135° C. (hexane/methylene chloride) and the corresponding compounds of Formula I-ZA-M2 as identified in the following table.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05633279 |
| Source dataset | uspto-grants-1997_05 |
| ORD ID | ord-78e66f63118845168ca11d31beeffab3 |
| Source note | uspto-grants-1997_05 |