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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1781533Generated: October 30, 2026

HCID 86750886, compound → HCID 70303321, compound

https://huagongshe.com/reaction/1781533

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 86750886HCID 86750886—
SolventMethylenechloride HexaneHCID 21226440—
ProductHCID 70303321HCID 70303321—

Reaction Steps

By following the procedure of Example ZA-6A and substituting methyl (E)-6-(1,3-dihydro-4-hydroxy-6-methoxy-7-methyl-3-oxoisobenzofuran-5-yl) 2,4-dimethyl-4-hexenoate with ethyl (E)-6-(1,3-dihydro-4-hydroxy-6-methoxy-7-methyl-3-oxoisobenzofuran-5-yl)-3-methoxy-4-methyl-4-hexenoate and the corresponding compounds of Formula I-ZA-M1 prepared as described in Part A above, there are obtained (E)-6-(1,3-dihydro-4-hydroxy-6-methoxy-7-methyl-3-oxoisobenzofuran-5-yl)-3-methoxy-4-methyl-4-hexenoic acid, m.p. 133°-135° C. (hexane/methylene chloride) and the corresponding compounds of Formula I-ZA-M2 as identified in the following table.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05633279
Source datasetuspto-grants-1997_05
ORD IDord-78e66f63118845168ca11d31beeffab3
Source noteuspto-grants-1997_05