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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1783384Generated: October 29, 2026

Dimethylamine → HCID 24759022, compound

https://huagongshe.com/reaction/1783384

Reaction equation

Participants

RoleNameHCIDCharge
ReactantDimethylamineHCID 674—
ReactantHCID 24759018HCID 24759018—
SolventEthanolHCID 702—
ProductHCID 24759022HCID 2475902299%

Reaction Steps

To a saturated solution of dimethylamine in ethanol (2 mL), cooled at 5° C. under Ar, was added 3-[4-[2-(4-fluoro-1H-indol-3-yl)-2-oxoacetyl]piperazin1-yl]-4-isopropoxy-cyclobut-3-ene-1,2-dione (0.020 g, 0.048 mmol) and the mixture was then allowed to stir at room temperature for 2 h. The volatiles were then removed in vacuo to give the essentially pure title compound (0.019 g, 99%) as a white solid:

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07501419B2
Source datasetuspto-grants-2009_03
ORD IDord-24fc9d4575e24c72add2703e98910e41
Source noteuspto-grants-2009_03