HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 68602341, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 68601928 | HCID 68601928 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 68602341 | HCID 68602341 | — |
Reaction Steps
To a solution of 95 in 1 mL dichloromethane was added 300 uL of TFA. The reaction was stirred for 1 hour and then concentrated in vacuo. The crude material was purified via reverse phase HPLC (C18, acetonitrile/water with 0.1% TFA) to yield 0.75 mg of 96. MS [M+H]+=446.0
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07501404B2 |
| Source dataset | uspto-grants-2009_03 |
| ORD ID | ord-4050746a657246f083fa41a02d1b514e |
| Source note | uspto-grants-2009_03 |