HuagongsheHuagongshe Chemistry Print Report · For research reference only
Nitric Acid → HCID 178469037, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Nitric Acid | HCID 944 | — |
| Reactant | Benzocaine | HCID 2337 | — |
| Reactant | Cyanamide | HCID 9864 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178469037 | HCID 178469037 | — |
Reaction Steps
4-aminobenzoic acid ethyl ester (20 g, 0.121 mol), nitric acid (7.26 g, 0.121 mol), cyanamide (50%, 14 ml 0.182 mol) were mixed under reflux with ethanol (50 ml). After 24 hr, the mixture was cooled to RT, and then washed with ethanol to give the titled compound as crystalline solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07501424B2 |
| Source dataset | uspto-grants-2009_03 |
| ORD ID | ord-c391bf99df534663a7c96a7ab4abfa3f |
| Source note | uspto-grants-2009_03 |