Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Iodine chloride | HCID 24640 | — |
| Reactant | HCID 57590528 | HCID 57590528 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 57590526 | HCID 57590526 | — |
Reaction Steps
A mixture of 4-benzoxazol-2-yl-piperazine-1-carboxylic acid benzyl ester (0.50 g, 1.48 mmol) and iodine monochloride (0.265 g, 1.63 mmol) in acetic acid (4.94 mL) was stirred at 60° C. overnight, cooled, and concentrated in vacuo to provide the title compound, which was used without further purification, in Example 3.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US07501421B2 |
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| Source dataset | uspto-grants-2009_03 |
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| ORD ID | ord-77e06490c243483cb610fca76a3fdc4f |
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| Source note | uspto-grants-2009_03 |
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