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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1783485Generated: October 29, 2026

Iodine chloride → HCID 57590526, compound

https://huagongshe.com/reaction/1783485

Reaction equation

Participants

RoleNameHCIDCharge
ReactantIodine chlorideHCID 24640—
ReactantHCID 57590528HCID 57590528—
SolventAcetic AcidHCID 176—
ProductHCID 57590526HCID 57590526—

Reaction Conditions

Temperature60 °C

Reaction Steps

A mixture of 4-benzoxazol-2-yl-piperazine-1-carboxylic acid benzyl ester (0.50 g, 1.48 mmol) and iodine monochloride (0.265 g, 1.63 mmol) in acetic acid (4.94 mL) was stirred at 60° C. overnight, cooled, and concentrated in vacuo to provide the title compound, which was used without further purification, in Example 3.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07501421B2
Source datasetuspto-grants-2009_03
ORD IDord-77e06490c243483cb610fca76a3fdc4f
Source noteuspto-grants-2009_03