Chloroacetonitrile → HCID 68859728, compound

HRID 1783498Notes

Reaction equation

HRID 1783498 reaction equation
[NH2:1][C:2]1[CH:7]=[CH:6][CH:5]=[C:4]([CH3:8])[C:3]=1[C:9](=O)[CH3:10].[Cl:12][CH2:13][C:14]#[N:15]>O1CCOCC1.Cl>[Cl:12][CH2:13][C:14]1[N:15]=[C:9]([CH3:10])[C:3]2[C:2](=[CH:7][CH:6]=[CH:5][C:4]=2[CH3:8])[N:1]=1

Participants

5

Reactant 2

HCID 7856ChloroacetonitrileHCID 142022571-(2-Amino-6-methylphenyl)ethanone

Product 1

HCID 68859728HCID 68859728, compound

Reagents, catalysts & solvents 2

HCID 313Hydrochloric AcidSolventHCID 312751,4-DioxaneSolvent

Procedure

Prepared by reacting 1-(2-amino-6-methyl-phenyl)-ethanone with chloroacetonitrile in dioxane while piping in hydrogen chloride at 30-38° C.

Workup

  1. customPrepared

Sources & evidence

ORD record
ord-dccd644595f345ec96dcc6a036f4cd13
Source dataset
uspto-grants-2009_03
Patent number
US07501426B2

Reaction notes

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