Triethylamine → HCID 86070947, compound

HRID 1783501Notes

Reaction equation

HRID 1783501 reaction equation
[OH:1][CH2:2][C:3]1[O:7][C:6]([CH:8]=[O:9])=[CH:5][CH:4]=1.[CH3:10][S:11](Cl)(=[O:13])=[O:12].C(N(CC)CC)C>C(Cl)Cl>[CH3:10][S:11]([O:1][CH2:2][C:3]1[O:7][C:6]([CH:8]=[O:9])=[CH:5][CH:4]=1)(=[O:13])=[O:12]

Participants

5

Reactant 3

HCID 8471TriethylamineHCID 31297Methanesulfonyl chlorideHCID 2373325-(Hydroxymethyl)furfural

Product 1

HCID 86070947HCID 86070947, compound

Reagents, catalysts & solvents 1

HCID 6344DichloromethaneSolvent

Procedure

Prepared by reacting 5-(hydroxymethyl)-2-furan-carboxaldehyde with methanesulfonic acid chloride in the presence of triethylamine in methylene chloride at ambient temperature. The crude product is further reacted without any more purification.

Workup

  1. customPrepared
  2. customat ambient temperature

Sources & evidence

ORD record
ord-e7688ff2973049e0bc24eed85ceeaad1
Source dataset
uspto-grants-2009_03
Patent number
US07501426B2

Reaction notes

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