huagongshe.com
HRID1784065

反应详情

EQUATION

反应方程式

HRID 1784065 的结构方程式

REACTANTS

反应物

2
结构：COc1cccc(C)c1N
HCID459249

2-Methoxy-6-methylaniline

C8H11NO

结构：COc1ccc2c(c1)CCn1c-2cc(Cl)nc1=O
HCID57591093

未命名化合物

PRODUCTS

生成物

1
结构：COc1ccc2c(c1)CCn1c-2cc(Nc2c(C)cccc2OC)nc1=O
HCID11439895

未命名化合物

PROCEDURE

实验过程

The title compound was prepared from 2-chloro-9-methoxy-6,7-dihydro-pyrimido[6,1-a]isoquinolin-4-one (4) and 2-methoxy-6-methyl-aniline as in Example 1 d. 1H-NMR (400 MHz, d6-DMSO) δ 8.71 (br, 1H), 7.71 (br, 1H), 7.35-6.80 (5H), 6.39 (br, 1H), 3.92 (br, 2H), 3.83 (br, 3H), 3.74 (br, 3H), 2.94 (t, 2H) and 2.14 (br, 3H); MS (ESI) (M+H)+ 364.