HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl 3-aminobenzoate → HCID 57591101, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl 3-aminobenzoate | HCID 11400 | — |
| Reactant | 2-chloro-9-methoxy-6,7-dihydro-4H-pyrimido[6,1-a]isoquinolin-4-one | HCID 57591093 | — |
| Product | HCID 57591101 | HCID 57591101 | — |
Reaction Steps
The title compound was prepared from 2-chloro-9-methoxy-6,7-dihydro-pyrimido[6,1-a]isoquinolin-4-one (4) and 3-amino-benzoic acid ethyl ester as in Example 1 d. 1H-NMR (400 MHz, d0-DMSO) δ 9.84 (s, 1H), 8.26 (s, 1H), 8.21 (d, 1H), 7.70 (d, 1H), 7.62 (d, 1H), 7.49 (t, 1H), 7.05-6.97 (2H), 6.36 (s, 1H), 4.33 (q, 2H), 3.99 (t, 2H), 3.85 (s, 3H), 2.97 (t, 2H) and 1.34 (t, 3H); MS (ESI) (M+H)+ 392.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07501512B2 |
| Source dataset | uspto-grants-2009_03 |
| ORD ID | ord-d9f835ed430e4e08ae863940294eabf6 |
| Source note | uspto-grants-2009_03 |