HuagongsheHuagongshe Chemistry Print Report · For research reference only
(3-Bromophenoxy)(tert-butyl)dimethylsilane → 7-(3-t-Butyldimethysilyloxyphenylsulfonyl)-1,2,4,5-tetrahydro-3-benzazepine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (3-Bromophenoxy)(tert-butyl)dimethylsilane | HCID 11254705 | — |
| Reactant | 3-Trifluoroacetyl-1,2,4,5-tetrahydro-3-benzazepine-7-sulfonyl fluoride | HCID 57592483 | — |
| Product | 7-(3-t-Butyldimethysilyloxyphenylsulfonyl)-1,2,4,5-tetrahydro-3-benzazepine | HCID 68859504 | 80% |
Reaction Steps
Prepared from 3-trifluoroacetyl-2,3,4,5-tetrahydro-1H-3-benzazepine-7-sulfonyl fluoride and 3-t-butyldimethylsilyloxybromobenzene using the method of Example 1, yield 80%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07504392B2 |
| Source dataset | uspto-grants-2009_03 |
| ORD ID | ord-cfc0c3931452434e99dfef546e8575c2 |
| Source note | uspto-grants-2009_03 |