HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 53628935, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 53628936 | HCID 53628936 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 53628935 | HCID 53628935 | 178.3% |
Reaction Steps
4N Hydrogen chloride in ethyl acetate was added to the solution of 2-(1-(tert-butoxycarbonyl)-2-(4-chlorophenyl)-piperazine-4-yl)-3-methyl-6-(4-pyridyl)pyrimidin-4-one (500 mg, 1.0 mmol) in ethyl acetate and stirred. Filtration and successive dryness gave the title compound (373 mg, 79%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07504411B2 |
| Source dataset | uspto-grants-2009_03 |
| ORD ID | ord-1c696d5240cc431587d259cc68331a13 |
| Source note | uspto-grants-2009_03 |