Bromopinacolone → HCID 86032942, compound

HRID 1784726Notes

Reaction equation

HRID 1784726 reaction equation
Br[CH2:2][C:3](=O)[C:4]([CH3:7])([CH3:6])[CH3:5].[NH2:9][C:10]1[CH:15]=[CH:14][C:13]([N+:16]([O-:18])=[O:17])=[CH:12][N:11]=1>C(OCC)(=O)C>[C:4]([C:3]1[N:9]=[C:10]2[CH:15]=[CH:14][C:13]([N+:16]([O-:18])=[O:17])=[CH:12][N:11]2[CH:2]=1)([CH3:7])([CH3:6])[CH3:5]

Participants

4

Reactant 2

HCID 21642BromopinacoloneHCID 778882-Amino-5-nitropyridine

Product 1

HCID 86032942HCID 86032942, compound

Reagents, catalysts & solvents 1

HCID 8857Ethyl AcetateSolvent

Procedure

Operations similar to Production Example 1-(2) were conducted using 1-bromopinacolone and 2-amino-5-nitropyridine. The solid whereupon obtained was suspended in ethyl acetate, and washed with saturated aqueous sodium hydrogencarbonate solution to provide the title compound as yellow solid.

Workup

  1. customThe solid whereupon obtained
  2. washwashed with saturated aqueous sodium hydrogencarbonate solution

Sources & evidence

ORD record
ord-07aff546efab4ea98c8878d08510434b
Source dataset
uspto-grants-2009_03
Patent number
US07504412B2

Reaction notes

Loading…