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HRID1784730

反应详情

EQUATION

反应方程式

HRID 1784730 的结构方程式

REACTANTS

反应物

2
反应SMILES：CCOC(=O)C(=O)CBr
HCID66144

Propanoic acid, 3-bromo-2-oxo-, ethyl ester

C5H7BrO3

反应SMILES：Nc1ccc([N+](=O)[O-])cn1
HCID77888

2-Pyridinamine, 5-nitro-

C5H5N3O2

PRODUCTS

产物

1
反应SMILES：CCOC(=O)c1cn2cc([N+](=O)[O-])ccc2n1
HCID12558381

Ethyl 6-nitroimidazo[1,2-a]pyridine-2-carboxylate

C10H9N3O4

AUXILIARIES

试剂、催化剂与溶剂

1
反应SMILES：CCOC(C)=O
溶剂HCID8857

Ethyl acetate

C4H8O2

PROCEDURE

实验过程

Operations similar to Production Example 1-(2) were conducted using ethyl bromopyruvate and 2-amino-5-nitropyridine. The solid whereupon obtained was suspended in ethyl acetate, and washed with saturated aqueous sodium hydrogencarbonate to provide the title compound as brown solid.

WORKUP

后处理

  1. customThe solid whereupon obtained
  2. washwashed with saturated aqueous sodium hydrogencarbonate