HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Chlorocyclohexanone → HCID 23120546, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Chlorocyclohexanone | HCID 13203 | — |
| Reactant | 2-Amino-5-nitropyridine | HCID 77888 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 23120546 | HCID 23120546 | — |
Reaction Steps
Operations similar to Production Example 1-(2) were conducted using 2-chlorocyclohexanone and 2-amino-5-nitropyridine. The resulting solid was suspended in ethyl acetate, washed with saturated aqueous sodium hydrogencarbonate solution and purified by silica gel column chromatography (hexane/ethyl acetate=2/1) to provide the title compound as yellow crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07504412B2 |
| Source dataset | uspto-grants-2009_03 |
| ORD ID | ord-6c35de7734a0408eaf9404625f6f2ad4 |
| Source note | uspto-grants-2009_03 |