HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Aminophenol → HCID 57438531, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Aminophenol | HCID 403 | — |
| Reactant | 2-Chloro-4-methoxypyridine | HCID 1991128 | — |
| Reactant | Potassium tert-butoxide | HCID 23665647 | — |
| Solvent | Dimethylacetamide | HCID 31374 | — |
| Product | HCID 57438531 | HCID 57438531 | — |
Reaction Steps
4-Aminophenol was reacted with 4-methoxy-2-chloropyridine in the presence of KOtBu/8-Crown-6/DMA at 150° C. for 5 hrs to give 2-(4-aminophenoxy)-4-methoxypyridine. The product was purified by chromatography.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07504416B2 |
| Source dataset | uspto-grants-2009_03 |
| ORD ID | ord-5e378f173bb444b7aee359cc610c6e24 |
| Source note | uspto-grants-2009_03 |