3-Aminopyridine → HCID 50994188, compound

HRID 1784866Notes

Reaction equation

HRID 1784866 reaction equation
[NH2:1][C:2]1[CH:3]=[N:4][CH:5]=[CH:6][CH:7]=1.[Br:8][C:9]1[CH:14]=[C:13](Br)[CH:12]=[C:11]([Br:16])[CH:10]=1>>[Br:8][C:9]1[CH:14]=[C:13]([NH:1][C:2]2[CH:3]=[N:4][CH:5]=[CH:6][CH:7]=2)[CH:12]=[C:11]([Br:16])[CH:10]=1

Participants

3

Reactant 2

HCID 100093-AminopyridineHCID 122791,3,5-Tribromobenzene

Product 1

HCID 50994188HCID 50994188, compound

Procedure

3-Aminopyridine was coupled with 1,3,5-tribromobenzene to give (3,5-dibromo-phenyl)-pyridin-3-yl-amine by the method described in Example 44. The reaction was complete in 1 hour. The dibromide was converted to N-[3-bromo-5-(pyridin-3-ylamino)-phenyl]-acetamide by the method of Example 82.

Sources & evidence

ORD record
ord-47da3b62b0ca484182c331a20b832d04
Source dataset
uspto-grants-2009_03
Patent number
US07504401B2

Reaction notes

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