HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl isocyanate → HCID 135828227, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl isocyanate | HCID 8022 | — |
| Reactant | HCID 135828224 | HCID 135828224 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 135828227 | HCID 135828227 | — |
Reaction Steps
62.2 mg (0.2 mmol) of 2-amino-6-[(2-aminoethyl)sulfanyl]-4-(4-hydroxyphenyl)-3,5-pyridinedicarbonitrile are suspended in 0.4 ml of DMF, and 14.2 mg (0.2 mmol) of ethyl isocyanate are added at room temperature. The mixture is stirred overnight, filtered and purified by preparative HPLC.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07504421B2 |
| Source dataset | uspto-grants-2009_03 |
| ORD ID | ord-fc5e0ee4c1fd4e79a84df5f3682c463b |
| Source note | uspto-grants-2009_03 |