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HRID1784915

反应详情

EQUATION

反应方程式

HRID 1784915 的结构方程式

REACTANTS

反应物

2
结构：N#CCC#N
HCID8010

Malononitrile

C3H2N2

结构：CC(=O)Nc1ccc(C=O)cc1
HCID73942

Acetamide, N-(4-formylphenyl)-

C9H9NO2

PRODUCTS

生成物

1
结构：CC(=O)Nc1ccc(C=C(C#N)C#N)cc1
HCID33296

Acetanilide, 4'-(2,2-dicyanovinyl)-

C12H9N3O

AUXILIARIES

试剂、催化剂与溶剂

2
结构：C1CCNCC1
催化剂HCID8082

Piperidine

C5H11N

结构：CCO
溶剂HCID702

Ethanol

C2H6O

PROCEDURE

实验过程

32.6 g (0.2 mol) of 4-acetaminobenzaldehyde and 13.74 g (0.208 mol) of malononitrile are initially charged in 140 ml of ethanol, and 24 drops of piperidine are added. The mixture is stirred at reflux for 30 min. After cooling, the crystals are filtered off with suction and dried.

WORKUP

后处理

  1. temperatureat reflux for 30 min
  2. temperatureAfter cooling
  3. filtrationthe crystals are filtered off with suction
  4. customdried