HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Methoxy-4-methylbenzaldehyde → 3-(3-Methoxy-4-methylphenyl)acrylonitrile
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Methoxy-4-methylbenzaldehyde | HCID 4715095 | — |
| Reactant | HCID 178511462 | HCID 178511462 | — |
| Product | 3-(3-Methoxy-4-methylphenyl)acrylonitrile | HCID 68959012 | 77% |
Reaction Steps
Wittig reaction of 3-methoxy-4-methylbenzaldehyde with cyanomethyl triphenylphosphorane gave 3-(3-methoxy-4-methylphenyl)acrylonitrile in 77% yield which was further transformed to 3-(3-methoxy-4-methylphenyl)propan-1-amine using the above described procedures.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07504420B2 |
| Source dataset | uspto-grants-2009_03 |
| ORD ID | ord-a5fc16ce1d4c41b2a9a42a400362c159 |
| Source note | uspto-grants-2009_03 |