HuagongsheHuagongshe Chemistry Print Report · For research reference only
Bromine → HCID 57431966, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Bromine | HCID 24408 | — |
| Reactant | Ethyl 2-(4-hydroxyphenoxy)acetate | HCID 13187337 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 57431966 | HCID 57431966 | — |
Reaction Steps
To a solution of (4-hydroxy-phenoxy)-acetic acid ethyl ester (0.59 g, 3 mmol) in acetic acid (1.5 mL) is added bromine (0.48 g, 9 mmol) in acetic acid (0.5 mL) at room temperature. After 5 min, solvent is evaporated and purified by column chromatography on silica gel giving the title compound (0.6 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07504433B2 |
| Source dataset | uspto-grants-2009_03 |
| ORD ID | ord-2996f51cb4824f62892a991a94ea41bc |
| Source note | uspto-grants-2009_03 |