HuagongsheHuagongshe Chemistry Print Report · For research reference only
[3-Isopropenyl-5-(4-trifluoromethyl-phenyl)-thiophen-2-yl]-methanol → HCID 57594995, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | [3-Isopropenyl-5-(4-trifluoromethyl-phenyl)-thiophen-2-yl]-methanol | HCID 68853480 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Product | HCID 57594995 | HCID 57594995 | — |
Reaction Steps
The solution of [3-Isopropenyl-5-(4-trifluoromethyl-phenyl)-thiophen-2-yl]-methanol (0.084 g, 0.282 mmole) is stirred under nitrogen gas in presence of 10% palladium on carbon (0.085 g) for 16 hours. The catalyst is removed by filtration, and the filtrate is concentrated to provide the titled compound as white solid, which is used for the next step without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07504433B2 |
| Source dataset | uspto-grants-2009_03 |
| ORD ID | ord-c911797e2cd04532ac685195fda962e8 |
| Source note | uspto-grants-2009_03 |