HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → (3-Nitrophenyl)urea
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | 3-Nitrophenyl isocyanate | HCID 76835 | — |
| Product | (3-Nitrophenyl)urea | HCID 3400496 | — |
Reaction Steps
Ammonia was bubbled into a solution of 3-nitrophenylisocyanate (1.5 g, 9.1 mmol) for ten minutes. The reaction mixture was then concentrated and the resulting yellow solid was washed with ether (200 mL) to afford N-(3-nitrophenyl)-urea (1.35 g, 7.5 mmol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07504410B2 |
| Source dataset | uspto-grants-2009_03 |
| ORD ID | ord-72664d7b391f4e4499752a268ef7893b |
| Source note | uspto-grants-2009_03 |