HRID1785311

反应详情

EQUATION

反应方程式

HRID 1785311 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

A solution of 3-(3-nitrophenyl)-2,4-imidazolidinedione (4.4 g, 20 mmol) and methanol (100 mL) was treated with 10% Pd/C (1.0 g) and placed under H2 (40 psi) for 2 h. The mixture was then filtered through celite and concentrated to afford the title compound (3.8 g).

WORKUP

后处理

  1. filtrationThe mixture was then filtered through celite
  2. concentrationconcentrated