HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-(3-Nitrophenyl)imidazolidine-2,4-dione → 3-(3-Aminophenyl)imidazolidine-2,4-dione
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-(3-Nitrophenyl)imidazolidine-2,4-dione | HCID 17352801 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 3-(3-Aminophenyl)imidazolidine-2,4-dione | HCID 24688437 | 99.4% |
Reaction Steps
A solution of 3-(3-nitrophenyl)-2,4-imidazolidinedione (4.4 g, 20 mmol) and methanol (100 mL) was treated with 10% Pd/C (1.0 g) and placed under H2 (40 psi) for 2 h. The mixture was then filtered through celite and concentrated to afford the title compound (3.8 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07504410B2 |
| Source dataset | uspto-grants-2009_03 |
| ORD ID | ord-9a14981d6c4d40c19cd39b640375616d |
| Source note | uspto-grants-2009_03 |