HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-[4-(1-tert-Butoxycarbonylamino-ethyl)-phenyl]-acrylic acid ethyl ester → HCID 69066102, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-[4-(1-tert-Butoxycarbonylamino-ethyl)-phenyl]-acrylic acid ethyl ester | HCID 69064356 | — |
| Catalyst | Palladium hydroxide | HCID 9942167 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 69066102 | HCID 69066102 | — |
Reaction Steps
Through a mixture of 3-[4-(1-tert-butoxycarbonylamino-ethyl)-phenyl]-acrylic acid ethyl ester (0.22 g, 0.69 mmol) and palladium hydroxide on carbon (100 mg) in ethanol (10 mL) was bubbled hydrogen through a balloon for 17 h. The mixture was filtered through celite and concentrated to afford an off-white solid. M+1=322.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07504403B2 |
| Source dataset | uspto-grants-2009_03 |
| ORD ID | ord-03202a9215ad4d28aa44793bae1ae8ea |
| Source note | uspto-grants-2009_03 |