反应详情

Through a mixture of 3-[4-(1-tert-butoxycarbonylamino-ethyl)-phenyl]-acrylic acid ethyl ester (0.22 g, 0.69 mmol) and palladium hydroxide on carbon (100 mg) in ethanol (10 mL) was bubbled hydrogen through a balloon for 17 h. The mixture was filtered through celite and concentrated to afford an off-white solid. M+1=322.

1. customwas bubbled hydrogen through a balloon for 17 h
2. filtrationThe mixture was filtered through celite
3. concentrationconcentrated
4. customto afford an off-white solid