HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(Methylthio)benzaldehyde → 2-(Trifluoromethyl)-4'-(methylthio)benzhydrol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(Methylthio)benzaldehyde | HCID 76985 | — |
| Reactant | (4-Chloro-2-(trifluoromethyl)phenyl)(phenyl)methanol | HCID 68907806 | — |
| Reactant | HCID 178506141 | HCID 178506141 | — |
| Product | 2-(Trifluoromethyl)-4'-(methylthio)benzhydrol | HCID 49962978 | — |
Reaction Steps
This material was prepared from 2-(trifluoromethyl)phenylmagnesium bromide (32 mmol) and 4-(methylthio)benzaldehyde (30 mmol) using the procedure described for compound (96) (9.4 g, 100%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07504522B2 |
| Source dataset | uspto-grants-2009_03 |
| ORD ID | ord-5f98a6e397b64cbb9a2ba9d641d66853 |
| Source note | uspto-grants-2009_03 |