HRID1785708

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID68902343

未命名化合物

结构：Fc1ccc(C(OC2CN(C(c3ccccc3)c3ccccc3)C2)c2ccccc2C(F)(F)F)cc1

HCID68903208

未命名化合物

PRODUCTS

生成物

结构：Cl.Fc1ccc(C(OC2CNC2)c2ccccc2C(F)(F)F)cc1

HCID68905655

未命名化合物

收率 55%

PROCEDURE

实验过程

This material was prepared from 1-benzhydryl-3-[2-(trifluoromethyl)-4′-fluorobenzyloxy]azetidine (161) (7.5 mmol) using the procedure described for compound (9). Crystallisation from DIPE-MeOH afforded the product as a white solid (1.49 g, 55%).

WORKUP

后处理

customCrystallisation from DIPE-MeOH