1-Bromooctane → HCID 22730205, compound

HRID 1785830Notes

Reaction equation

[Br:1][C:2]1[C:3]([CH3:8])=[N:4][NH:5][C:6]=1[CH3:7].Br[CH2:10][CH2:11][CH2:12][CH2:13][CH2:14]CCC.IC1C=NNC=1>>[Br:1][C:2]1[C:3]([CH3:8])=[N:4][N:5]([CH2:10][CH2:11][CH2:12][CH2:13][CH3:14])[C:6]=1[CH3:7]

Participants

Reactant 3

HCID 81401-Bromooctane

HCID 769374-bromo-3,5-dimethyl-1H-pyrazole

HCID 770224-Iodopyrazole

Product 1

HCID 22730205HCID 22730205, compound

Procedure

The desired product was prepared by substituting 5-iodopentane and 4-bromo-3,5-dimethylpyrazole for 1-bromooctane and 4-iodopyrazole, respectively, in Example 198A. MS (ESI(+)) m/e 245, 247 (M+H)+.

Sources & evidence

ORD record: ord-554ed541d6be487298a4a9d55a3a6081
Source dataset: uspto-grants-2009_03
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US07504512B2

Reaction notes

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