HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Chloro-2-methylbenzenesulfonyl chloride → 3-Chloro-N-(2-ethyl-pyrimidin-4-yl)-2-methyl-benzenesulfonamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Chloro-2-methylbenzenesulfonyl chloride | HCID 522734 | — |
| Reactant | 2-Ethyl-4-pyrimidinamine | HCID 13925296 | — |
| Product | 3-Chloro-N-(2-ethyl-pyrimidin-4-yl)-2-methyl-benzenesulfonamide | HCID 11623768 | — |
Reaction Steps
This compound was obtained according to example 2, step B] from 2-ethyl-pyrimidin-4-ylamine (0.25 g), and 3-chloro-2-methyl-benzenesulfonyl chloride (0.55 g) as a colorless solid (86 mg). MS (ESI−): 310.0 ([M−H]−).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07507733B2 |
| Source dataset | uspto-grants-2009_03 |
| ORD ID | ord-3b73d4d4d4ee41bfa2cbeea7f5c4bc2a |
| Source note | uspto-grants-2009_03 |