HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Chloro-2-methylbenzenesulfonyl chloride → 3-Chloro-N-(2-cyclobutyl-pyrimidin-4-yl)-2-methyl-benzenesulfonamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Chloro-2-methylbenzenesulfonyl chloride | HCID 522734 | — |
| Reactant | 2-Cyclobutylpyrimidin-4-amine | HCID 45787578 | — |
| Product | 3-Chloro-N-(2-cyclobutyl-pyrimidin-4-yl)-2-methyl-benzenesulfonamide | HCID 11573626 | — |
Reaction Steps
This compound was obtained according to example 2, step B] from 2-cyclobutyl-pyrimidin-4-ylamine (0.15 g), and 3-chloro-2-methyl-benzenesulfonyl chloride (0.27 g) as a light brown solid (47 mg). MS (ESI): 338.1 (MH+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07507733B2 |
| Source dataset | uspto-grants-2009_03 |
| ORD ID | ord-c1ad65b5ed734f73a3282ffb2f81586a |
| Source note | uspto-grants-2009_03 |