HuagongsheHuagongshe Chemistry Print Report · For research reference only
9-chloro-2-cyclopropyl-6H-[1,2,4]triazolo[1,5-c]quinazolin-5-one → HCID 178494724, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 9-chloro-2-cyclopropyl-6H-[1,2,4]triazolo[1,5-c]quinazolin-5-one | HCID 136332316 | — |
| Reactant | 9-Chloro-2-methoxymethyl-6H-[1,2,4]triazolo[1,5-c]quinazolin-5-one | HCID 136347869 | — |
| Product | HCID 178494724 | HCID 178494724 | 92.3% |
Reaction Steps
As described for example 1b) 9-chloro-2-methoxymethyl-6H-[1,2,4]triazolo[1,5-c]quinazolin-5-one (73.4 g, 277 mmol), instead of 9-chloro-2-cyclopropyl-6H-[1,2,4]triazolo[1,5-c]quinazolin-5-one, was converted to the title compound (61.0 g, 92%) which was obtained as a brown solid. MS: m/e=238.9 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07507729B2 |
| Source dataset | uspto-grants-2009_03 |
| ORD ID | ord-572e832a6c0e4cea9e047c688cfc995b |
| Source note | uspto-grants-2009_03 |