HuagongsheHuagongshe Chemistry Print Report · For research reference only
9-chloro-2-cyclopropyl-6H-[1,2,4]triazolo[1,5-c]quinazolin-5-one → HCID 178494721, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 9-chloro-2-cyclopropyl-6H-[1,2,4]triazolo[1,5-c]quinazolin-5-one | HCID 136332316 | — |
| Reactant | 9-Bromo-2-methoxymethyl-6H-[1,2,4]triazolo[1,5-c]quinazolin-5-one | HCID 136332328 | — |
| Product | HCID 178494721 | HCID 178494721 | 99.8% |
Reaction Steps
As described for example 1b) 9-bromo-2-methoxymethyl-6H-[1,2,4]triazolo[1,5-c]quinazolin-5-one (20.9 g, 67.6 mmol), instead of 9-chloro-2-cyclopropyl-6H-[1,2,4]triazolo[1,5-c]quinazolin-5-one, was converted to the title compound (19.1 g, 99%) which was obtained as an off-white solid. MS: m/e=282.7/284.7 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07507729B2 |
| Source dataset | uspto-grants-2009_03 |
| ORD ID | ord-a04a2da259b64d18a20cf3563a9b9544 |
| Source note | uspto-grants-2009_03 |