HCID 178494720, compound → 9-Bromo-2-methoxymethyl-6H-1,3,3a,6-tetraaza-benzo[e]azulen-5-one

Participants

Reaction Steps

As described for example 4d) 2-chloro-N-[4-bromo-2-(5-methoxymethyl-2H-[1,2,4]triazol-3-yl)-phenyl]-acetamide (20.6 g, 57.3 mmol), instead of 2-chloro-N-[4-chloro-2-(5-methoxymethyl-2H-[1,2,4]triazol-3-yl)-phenyl]-acetamide, was converted to the title compound (12.6 g, 68%) which was obtained as an off-white solid. MS: m/e=322.0/324.0 [M+H]+.

Provenance & Evidence