HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrazine hydrate (1:1) → HCID 45119106, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrazine hydrate (1:1) | HCID 24654 | — |
| Reactant | methyl 3,3,3-trifluoro-dl-lactate | HCID 2760118 | — |
| Solvent | 1-Butanol | HCID 263 | — |
| Product | HCID 45119106 | HCID 45119106 | — |
Reaction Steps
As described for example 112a, methyl-3,3,3-trifluoro-DL-lactate in butanol was reacted with hydrazine hydrate (1.2 equivalents) at rt for 16 h. The mixture was concentrated and the title compound was obtained as a light yellow oil (yield: 81%). MS: m/e=158.0 [M]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07507729B2 |
| Source dataset | uspto-grants-2009_03 |
| ORD ID | ord-3ed0c45c9a6c4e9cb8a5baa9d1aa71a3 |
| Source note | uspto-grants-2009_03 |