Methyl iodide → HCID 11179318, compound

Participants

Reaction Steps

The title compound was prepared from 2-benzyl-1-(8-methyl-8-aza-bicyclo[3.2.1]oct-3-ylidene)-3-phenyl-propan-2-ol and methyliodide by following the experimental procedures in Example 4 (85% yield): LCMS (ES) m/z 346 (M+H)+; 1H-NMR(CDCl3) δ 0.80 (m, 1H), 1.48 (m, 1H), 1.84 (m, 1H), 1.99 (m, 1H), 2.09 (m, 2H), 2.87 (m, 1H), 2.95 (m, 5H), 3.16 (s, 3H), 3.26 (s, 3H), 4.16 (m, 1H), 4.18 (m, 1H), 5.42 (s, 1H), 7.26 (m, 10H).

Provenance & Evidence