Methyl iodide → HCID 11374612, compound

Participants

Reaction Steps

The title compound was prepared from 2-(8-methyl-8-aza-bicyclo[3.2.1]oct-3-ylidene)-1,1-diphenyl-ethanol and methyliodide by following the experimental procedures in Example 4 (67% yield): LCMS (ES) m/z 334 (M+H)+; 1H-NMR(CDCl3) δ 1.50 (m, 1H), 1.98 (m, 1H), 2.11 (m, 1H), 2.35 (m, 2H), 2.87 (m, 1H), 2.96 (m, 1H), 3.23 (m, 1H), 3.27 (s, 3H), 3.56 (s, 3H), 4.00 (m, 1H), 4.28 (m, 1H), 6.49 (s, 1H), 7.35 (m, 8H), 7.49 (m, 2H).

Provenance & Evidence