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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1786541Generated: October 29, 2026

HCID 69053739, compound → HCID 57597584, compound

https://huagongshe.com/reaction/1786541

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 69053739HCID 69053739—
CatalystPalladiumHCID 23938—
SolventMethanolHCID 887—
ProductHCID 57597584HCID 57597584116.4%

Reaction Steps

To a solution of 3-benzhydryl-1-(1-benzoyl-pyrrolidin-3-yl)-1-methyl-urea (0.7 g, 1.75 mmol) in CH3OH (25 ml) was added Pd/C 20% (175 mg). The resulting slurry was hydrogenated at 50 psi for 24 hours. The catalyst was filtered through Celite and filtrate evaporated under reduced pressure to, give 0.63 g of desired product.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07507760B2
Source datasetuspto-grants-2009_03
ORD IDord-189f5f3cf8bb43dca2e6b5ca20960bd3
Source noteuspto-grants-2009_03