HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 69053739, compound → HCID 57597584, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 69053739 | HCID 69053739 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 57597584 | HCID 57597584 | 116.4% |
Reaction Steps
To a solution of 3-benzhydryl-1-(1-benzoyl-pyrrolidin-3-yl)-1-methyl-urea (0.7 g, 1.75 mmol) in CH3OH (25 ml) was added Pd/C 20% (175 mg). The resulting slurry was hydrogenated at 50 psi for 24 hours. The catalyst was filtered through Celite and filtrate evaporated under reduced pressure to, give 0.63 g of desired product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07507760B2 |
| Source dataset | uspto-grants-2009_03 |
| ORD ID | ord-189f5f3cf8bb43dca2e6b5ca20960bd3 |
| Source note | uspto-grants-2009_03 |