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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1786544Generated: October 29, 2026

HCID 69053132, compound → HCID 57597579, compound

https://huagongshe.com/reaction/1786544

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 69053132HCID 69053132—
CatalystPalladiumHCID 23938—
SolventMethanolHCID 887—
ProductHCID 57597579HCID 57597579114.1%

Reaction Steps

To a solution of (R)—N-(1-benzoyl-pyrrolidin-3-yl)-2-diphenylamino-N-methyl-acetamide (0.68 g, 1.7 mmol) in CH3OH (30 ml) was added Pd/C 20% (170 mg). The resulting slurry was hydrogenated at 50 psi for 24 hours. The catalyst was filtered through Celite and filtrate evaporated under reduced pressure to give 0.6 g of desired product.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07507760B2
Source datasetuspto-grants-2009_03
ORD IDord-e56469efe4574f2b8684abbf187dfa1c
Source noteuspto-grants-2009_03