Mandelic Acid → HCID 68705187, compound

HRID 1787168Notes

Reaction equation

HRID 1787168 reaction equation
[CH3:1][C:2]1[C:7]([CH3:8])=[CH:6][C:5]([CH3:9])=[CH:4][C:3]=1O.O[CH:12]([C:16]1[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=1)[C:13]([OH:15])=[O:14]>C(OCC)(=O)C.CCCCCC>[C:16]1([CH:12]2[C:4]3[C:5]([CH3:9])=[CH:6][C:7]([CH3:8])=[C:2]([CH3:1])[C:3]=3[O:15][C:13]2=[O:14])[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=1

Participants

4

Reactant 2

HCID 1292Mandelic AcidHCID 127692,3,5-Trimethylphenol

Product 1

HCID 68705187HCID 68705187, compoundYield 37%

Reagents, catalysts & solvents 1

HCID 21226206Ethyl acetate hexaneSolvent

Procedure

Using 2,3,5-trimethylphenol and hydroxy(phenyl)acetic acid, the title compound was synthesized in the same manner as in Reference Example 2. Yield 37%. Melting point: 129-130° C. (ethyl acetate-hexane).

Sources & evidence

ORD record
ord-2406c50f42984f69a1fee41857fc5967
Source dataset
uspto-grants-2009_03
Patent number
US07507841B2

Reaction notes

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