Phenacyl bromide → HCID 898257, compound

HRID 1787209Notes

Reaction equation

HRID 1787209 reaction equation
[CH3:1][C:2]1[CH:3]=[C:4]([OH:9])[CH:5]=[C:6]([CH3:8])[CH:7]=1.[CH2:10](Br)[C:11]([C:13]1[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1)=[O:12]>CO>[CH3:1][C:2]1[CH:3]=[C:4]([CH:5]=[C:6]([CH3:8])[CH:7]=1)[O:9][CH2:10][C:11]([C:13]1[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1)=[O:12]

Participants

4

Reactant 2

HCID 6259Phenacyl bromideHCID 79483,5-Dimethylphenol

Product 1

HCID 898257HCID 898257, compoundYield 86%

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

Using 3,5-dimethylphenol and phenacyl bromide, the title compound was synthesized in the same manner as in Reference Example 177. Yield 86%. Melting point: 104-105° C. (methanol).

Sources & evidence

ORD record
ord-02429486b0574ddb940d47953e93a712
Source dataset
uspto-grants-2009_03
Patent number
US07507841B2

Reaction notes

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