Ethyl Acetate → HCID 23114320, compound

HRID 1787246Notes

Reaction equation

[CH3:1][C:2]1[C:7]2[CH:8]([C:11]3[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=3)[CH2:9][O:10][C:6]=2[C:5]([CH3:17])=[C:4]([CH3:18])[C:3]=1[NH2:19].C([O:23][CH2:24][CH3:25])(=O)C>>[CH3:1][C:2]([CH3:7])([CH3:3])[CH2:25][C:24]([NH:19][C:3]1[C:4]([CH3:18])=[C:5]([CH3:17])[C:6]2[O:10][CH2:9][CH:8]([C:11]3[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=3)[C:7]=2[C:2]=1[CH3:1])=[O:23]

Participants

Reactant 2

HCID 8857Ethyl Acetate

HCID 68707870HCID 68707870, compound

Product 1

HCID 23114320HCID 23114320, compoundYield 50%

Procedure

Using 4,6,7-trimethyl-3-phenyl-2,3-dihydro-1-benzofuran-5-amine obtained in Reference Example 306, the title compound was synthesized in the same manner as in Example 1. Yield: 50%. Melting point: 146-147° C. (ethyl acetate).

Workup

customobtained in Reference Example 306

Sources & evidence

ORD record: ord-7f48851790fb44b19e91491c3ddacb67
Source dataset: uspto-grants-2009_03
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US07507841B2

Reaction notes

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