Ethyl Acetate → HCID 23114411, compound

HRID 1787247Notes

Reaction equation

[CH3:1][C:2]1[C:7]2[CH:8]([C:11]3[CH:16]=[CH:15][C:14]([CH3:17])=[CH:13][CH:12]=3)[CH2:9][O:10][C:6]=2[C:5]([CH3:18])=[C:4]([CH3:19])[C:3]=1[NH2:20].C([O:24][CH2:25][CH3:26])(=O)C>>[CH3:1][C:2]([CH3:7])([CH3:3])[CH2:26][C:25]([NH:20][C:3]1[C:4]([CH3:19])=[C:5]([CH3:18])[C:6]2[O:10][CH2:9][CH:8]([C:11]3[CH:16]=[CH:15][C:14]([CH3:17])=[CH:13][CH:12]=3)[C:7]=2[C:2]=1[CH3:1])=[O:24]

Participants

Reactant 2

HCID 8857Ethyl Acetate

HCID 68707832HCID 68707832, compound

Product 1

HCID 23114411HCID 23114411, compoundYield 80%

Procedure

Using 4,6,7-trimethyl-3-(4-methylphenyl)-2,3-dihydro-1-benzofuran-5-amine obtained in Reference Example 307, the title compound was synthesized in the same manner as in Example 1. Yield: 80%. Melting point: 176-177° C. (ethyl acetate).

Workup

customobtained in Reference Example 307

Sources & evidence

ORD record: ord-dbc21e3c322e472a927bb306def0822a
Source dataset: uspto-grants-2009_03
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US07507841B2

Reaction notes

Loading…