N,N-Dimethylethylenediamine → HCID 23114344, compound

HRID 1787298Notes

Reaction equation

HRID 1787298 reaction equation
[CH:1]([C:4]1[CH:9]=[CH:8][C:7]([CH:10]2[C:14]3[C:15]([CH3:30])=[C:16]([NH:21][C:22](=[O:29])OCC(Cl)(Cl)Cl)[C:17]([CH3:20])=[C:18]([CH3:19])[C:13]=3[O:12][CH2:11]2)=[CH:6][CH:5]=1)([CH3:3])[CH3:2].[CH3:31][N:32]([CH3:36])[CH2:33][CH2:34][NH2:35]>CCCCCC.C(OCC)(=O)C>[CH3:31][N:32]([CH3:36])[CH2:33][CH2:34][NH:35][C:22]([NH:21][C:16]1[C:17]([CH3:20])=[C:18]([CH3:19])[C:13]2[O:12][CH2:11][CH:10]([C:7]3[CH:6]=[CH:5][C:4]([CH:1]([CH3:2])[CH3:3])=[CH:9][CH:8]=3)[C:14]=2[C:15]=1[CH3:30])=[O:29]

Participants

4

Reactant 2

HCID 66053N,N-DimethylethylenediamineHCID 86618058HCID 86618058, compound

Product 1

HCID 23114344HCID 23114344, compoundYield 54%

Reagents, catalysts & solvents 1

HCID 21226206Ethyl acetate hexaneSolvent

Procedure

Using 2,2,2-trichloroethyl (3-(4-isopropylphenyl)-4,6,7-trimethyl-2,3-dihydro-1-benzofuran-5-yl)carbamate obtained in Example 138 and 2-(dimethylamino)ethylamine, the title compound was synthesized in the same manner as in Example 143. Yield: 54%. Melting point: 133-134° C. (hexane-ethyl acetate).

Sources & evidence

ORD record
ord-57265737341f45738149791b0c2c1a83
Source dataset
uspto-grants-2009_03
Patent number
US07507841B2

Reaction notes

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